By Yogesh M. Joshi, Sameer Khandekar
The e-book is an final result of study paintings within the components of nanotechnology, interfacial technological know-how, nano- and micro-fluidics and production, smooth topic, and delivery phenomena at nano- and micro-scales. The contributing authors signify sought after study teams from Indian Institute of know-how Bombay, Indian Institute of expertise Kanpur and Indian Institute of technology, Bangalore. The publication has thirteen chapters and the whole paintings provided within the chapters is predicated on examine performed over earlier 3 years. The chapters are designed with variety of colored illustrations, figures and tables. The e-book could be hugely worthy to academicians in addition to business execs operating within the pointed out areas.
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Additional info for Nanoscale and Microscale Phenomena: Fundamentals and Applications
7ı which can be indexed to (111), (200), (220), (222), (400), (420), and (422) planes of pure AgBr (JCPDF №. 79-0149) confirming the presence of AgBr particles . 75 nm. K. Gupta et al. Fig. 5 UV absorption spectra of AgBr nanoparticles varying with time. 8ı . These can be attributed to silver metallic particles (JCPDF №. 04-0783). Unlike Liu et al. , who proposed that complexes such as CTAB–AgBr are likely to form at higher surfactant concentration, we did not observe any signature of these complexes in the XRD pattern obtained in the present study (Fig.
11a). A time study revealed that nanospheres are formed after 1 h. At intermediate times, chain-like structures were observed, some of which showed signatures of consolidation, while at 24 h smoothened nanorods were observed (Fig. 11a). K. Gupta et al. Fig. 10 TEM image showing AgBr nanorods after 24 h. ŒCTAB D 50 mM, ŒAgNO3 D 10 mM, ŒNaSal D 100 mM (after 1 h) Fig. 11 Time study of AgBr nanorod synthesis, ŒCTAB D 50mM, ŒNaSal D 100 mM, and ŒAgNO3 D 10 mM. (a) AgBr nanoparticles at different time interval of aging.
The energy-dispersive X-ray spectroscopy (EDS) pattern of the synthesized AgBr nanoparticles is shown in Fig. 6. The spectrum shows the presence of bromine and silver elements. The peaks located between 2 and 4 keV are related to the silver characteristic lines while peaks located between 1 and 2 keV are related to the bromide characteristic lines. 5 keV represents the oxygen characteristic line. 75 keV appears in Fig. 6 because of the use of a silica wafer as a substrate for EDS analysis. To confirm the role of CTAB–NaSal wormlike templates on the shape of the anisotropic nanoparticles, the synthesis of AgBr was carried out in the absence of NaSal.